banner
Case

Water Contamination & Ice Blockage

Water Contamination & Ice Blockage
Diagnosis, physical separation, molecular sieve drying, and nitrogen blanketing protection for water-free coolant systems after water ingress. 6 real cases analyzed in depth.

6 Ice Blockage Cases
4 Water Removal Methods
5 Protection Design Steps

Water Contamination & Ice Blockage

Diagnosis, physical separation, molecular sieve drying, and nitrogen blanketing protection for water-free coolant systems after water ingress. 6 real cases analyzed in depth.

6 Ice Blockage Cases4 Water Removal Methods5 Protection Design Steps

Why Water-Free Coolants Fear Water

LM-11D, LM-11F, and other water-free coolants are designed specifically for ultra-low temperature applications. Their core advantage is the absence of water in the system. However, once moisture enters, it rapidly freezes at -40C to -60C low temperatures, causing pipe blockage, pump seizure, and localized heat exchanger icing - potentially leading to equipment damage.

2025 technical support data shows that LM-11D water ingress and ice blockage is the most frequent problem type, occurring 6 times in 34 typical cases, covering multiple water ingress pathways and ice blockage manifestations.

Main Water Ingress Pathways

  • Residual water in pipes not drained - after system cleaning or testing
  • Open tank admitting water - open tanks in contact with air, moisture condensation enters
  • Water used for pressure testing - water-prohibited systems mistakenly using water for leak testing
  • Air moisture condensation - moisture ingress at system openings in humid environments

Ice BlockageDiagnosis & Solutions

Pump Seizure & Pipe Blockage

Low-temperature moisture freezing causes pump seizure and pipe blockage. After temperature rises, ice melts and the pump restarts, but the problem is not resolved. Solution: Physical separation - let stand to stratify and collect upper coolant. Molecular sieve drying - treat residual moisture. Install filter before pump with regular cleaning based on operating current.

Cooling Difficulty & Moisture Detection

Moisture detected in system (e.g., 104 ppm), cannot cool below -40C. Plate heat exchanger locally iced, blocking heat transfer. Solution: Drain coolant and let stand to stratify, collecting upper portion. Thoroughly blow-dry system. Use dry nitrogen for pressure leak testing. Long-term: nitrogen blanketing and sealed tank.

Molecular Sieve Ineffective

Molecular sieve used but water removal is unsatisfactory, water content still high. Solution: Try adding alcohol to lower water freezing point (Beijing lab showed some effect). More thorough approach: physical separation followed by molecular sieve drying.

Leak Testing Water-Prohibited Systems

LM-11F and other water-prohibited systems cannot use water for pressure leak testing, as water will remain in the system. Solution: Use dry nitrogen for pressure leak testing to ensure the system has no leaks and no moisture residue.

Ice BlockageReal Cases

2025.02.18LM-11D
Baisheng · Shenzhen
LM-11D water contamination; ice blockage during cooling
System water tank open; previous LM-4 test not fully drained. Recommended draining coolant, stratifying, collecting upper portion, blow-drying system
2025.06.17LM-11D
Guangzhou Hengxing · Guangzhou
LM-11D ice blockage; pump seizes then restarts after temperature rises
Moisture reduced to 47ppm. Recommended filter before pump; clean regularly based on operating current
2025.07.02LM-11D
- · Inner Mongolia
LM-11D system reactor not receiving fluid
Suspected inlet pipe blockage or ice blockage. Drain coolant for physical density separation of water. Recommend nitrogen blanketing for tank
2025.09.21LM-11D
- · Chongqing
LM-11D water contamination ice blockage; molecular sieve ineffective
Tried adding alcohol to lower water freezing point; Beijing lab tests showed some effect; customer to try
2025.11.26LM-11D
Shanghai Nuoleng · -
LM-11D water contamination; cannot cool below -40°C; water content 104ppm
Recommended physical separation followed by molecular sieve drying
2025.12.03LM-11D/LM-8
- · Jiangsu
LM-11D replacing LM-8
Pipes to DN40/DN50, flow rate double, heat exchange area 1.5x

Anti-Ice BlockageSystem Design Essentials

Nitrogen Blanketing

Use nitrogen blanketing on the tank to isolate airborne moisture. This is the most effective measure to prevent water ingress in water-free coolant systems. Maintain nitrogen blanketing pressure at a slight positive pressure.

Sealed Tank Design

Use closed-loop tanks or sealed expansion tanks to avoid direct contact between open tanks and air. Position return lines at the bottom of the tank to reduce agitation and gas entrainment.

Dry Nitrogen Leak Testing

Water-prohibited systems must never use water for pressure leak testing. Always use dry nitrogen for pressure leak testing to ensure system tightness without introducing moisture.

Pre-Pump Filter

Install a filter before the pump to intercept precipitated crystals or ice crystals. Clean the filter regularly based on operating current changes to prevent blockage.

Water Content Monitoring

Regularly test coolant water content. LM-11D used below -40C should have water content controlled at extremely low levels (recommended below 50 ppm). Investigate water ingress sources immediately if water content increases.

Water Removal Method Comparison

Physical separation: Uses density difference; after standing, coolant and water stratify. Collect the upper coolant layer. Suitable for initial separation of large water volumes.
Molecular sieve drying: Treats trace residual moisture after physical separation. Note: effectiveness may be limited; use in combination with physical separation.
Alcohol freezing point depression: Add appropriate alcohol to lower water freezing point as a temporary emergency measure, not a long-term solution.
System blow-drying: Use dry nitrogen to purge system piping, removing residual moisture. Suitable for drying after system cleaning.

Ice BlockageFAQ

LM-11D system experiences ice blockage (pump seizure, pipe blockage)
Cause: LM-11D is a water-free coolant; moisture entering the system freezes at low temperatures causing ice blockage

Solution: Physical separation: let stand and stratify, collect upper coolant. Molecular sieve drying: use molecular sieves for residual moisture. Recommend nitrogen blanketing for water tank. Install filter before pump, clean regularly based on operating current
Moisture detected in system, cooling difficulties
Cause: Residual water in pipes not drained, open water tank intake, air moisture condensation

Solution: Drain coolant, let stand and stratify, collect upper portion. Thoroughly blow-dry system. Use dry nitrogen for pressure leak testing. Long-term: add nitrogen blanketing, seal water tank
How to test for leaks in water-prohibited systems like LM-11F
Cause: Water-prohibited systems cannot use water for pressure leak testing

Solution: Use dry nitrogen for pressure leak testing to ensure no leakage points

Post time: Aug-27-2026